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Encapsulation of exenatide in poly-(d,l-lactide- co -glycolide) microspheres produced an investigational long-acting once-weekly formulation for type 2 diabetes

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Chromatography was performed by injecting samples (3.5 l injection volume) onto an ACE EXCEL 2 C18-PFP 150 2.1 mm column (Avantor, EXL-1010-1502U), which was maintained at 30 C in the column compartment